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Publication Detail
High-resolution neutron-diffraction measurements to 8 kbar
  • Publication Type:
    Journal article
  • Publication Sub Type:
  • Authors:
    Bull CL, Fortes AD, Ridley CJ, Wood IG, Dobson DP, Funnell NP, Gibbs AS, Goodway CM, Sadykov R, Knight KS
  • Publication date:
  • Pagination:
    1, 9
  • Journal:
    High Pressure Research
  • Status:
  • Print ISSN:
© 2017 Informa UK Limited, trading as Taylor & Francis Group We describe the capability to measure high-resolution neutron powder diffraction data to a pressure of at least 8 kbar. We have used the HRPD instrument at the ISIS neutron source and a piston-cylinder design of pressure cell machined from a null-scattering titanium zirconium alloy. Data were collected under hydrostatic conditions from an elpasolite perovskite La(Formula presented.)NiMnO(Formula presented.); by virtue of a thinner cell wall on the incident-beam side of the cell, it was possible to obtain data in the instrument's highest resolution back-scattering detector banks up to a maximum pressure of 8.5 kbar.
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