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Publication Detail
High resolution 1H- and 13C-N.M.R spectra of D-glucopyranose, 2-acetamido-2-deoxy-D-glucopyranose, and related compounds in aqueous media
  • Publication Type:
    Journal article
  • Publication Sub Type:
    Journal Article
  • Authors:
    Perkins SJ, Johnson LN, Phillips DC, Dwek RA
  • Publication date:
  • Pagination:
    19, 34
  • Journal:
    Carbohydrate Research
  • Volume:
  • Issue:
  • Status:
  • Print ISSN:
The 1H- and 13C-n.m.r spectra of D-glucopyranose and 2-acetamido-2-deoxy-D-glucopyranose and its derivatives in D2O at 25° have been completely interpreted. Iterative analysis allowed accurate determination of the chemical shifts and coupling constants in the 270-MHz 1H-spectra, and these are used to correlate the chemical shift changes with substitution patterns. The implications of the systematic errors from assuming first-order conditions for the p.m.r spectra of sugars are discussed in relation to measuring shift changes of sugar-enzyme complexes. © 1977.
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