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Publication Detail
High resolution 1H- and 13C-N.M.R spectra of D-glucopyranose, 2-acetamido-2-deoxy-D-glucopyranose, and related compounds in aqueous media
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Publication Type:Journal article
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Publication Sub Type:Journal Article
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Authors:Perkins SJ, Johnson LN, Phillips DC, Dwek RA
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Publication date:01/01/1977
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Pagination:19, 34
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Journal:Carbohydrate Research
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Volume:59
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Issue:1
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Status:Published
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Print ISSN:0008-6215
Abstract
The 1H- and 13C-n.m.r spectra of D-glucopyranose and 2-acetamido-2-deoxy-D-glucopyranose and its derivatives in D2O at 25° have been completely interpreted. Iterative analysis allowed accurate determination of the chemical shifts and coupling constants in the 270-MHz 1H-spectra, and these are used to correlate the chemical shift changes with substitution patterns. The implications of the systematic errors from assuming first-order conditions for the p.m.r spectra of sugars are discussed in relation to measuring shift changes of sugar-enzyme complexes. © 1977.
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