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Publication Detail
Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques
  • Publication Type:
    Journal article
  • Publication Sub Type:
    Article
  • Authors:
    Simmance K, Sankar G, Bell RG, Prestipino C, van Beek W
  • Publisher:
    ROYAL SOC CHEMISTRY
  • Publication date:
    2010
  • Pagination:
    559, 562
  • Journal:
    PHYS CHEM CHEM PHYS
  • Volume:
    12
  • Issue:
    3
  • Print ISSN:
    1463-9076
  • Language:
    EN
  • Keywords:
    HYDROTHERMAL SYNTHESIS, POWDER DIFFRACTION, CRYSTALLIZATION, ZEOLITES, CATALYST, TIME, ALUMINOPHOSPHATES, MECHANISM, COAPO-5, XRD
  • Addresses:
    Sankar, G
    UCL
    Dept Chem
    London
    WC1H 0AJ
    England

    Univ Piemonte Orientale
    Dipartimento Sci & Tecnol Avanzate
    I-15100
    Alessandria
    Italy
Abstract
We followed the formation of metal ion substituted aluminophosphate, a redox molecular sieve, using a newly developed in situ simultaneous X-ray diffraction and X-ray absorption spectroscopic technique. The study showed that a cobalt-phosphorous network forms prior to the crystallisation.
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