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Publication Detail
Spectroscopic studies of sulfite-based polyoxometalates at high temperature and high pressure
  • Publication Type:
    Journal article
  • Publication Sub Type:
    Journal Article
  • Authors:
    Quesada Cabrera R, Firth S, Blackman CS, Long DL, Cronin L, McMillan PF
  • Publication date:
  • Pagination:
    171, 176
  • Journal:
    Journal of Solid State Chemistry
  • Volume:
  • Status:
  • Print ISSN:
Structural changes occurring within non-conventional Dawson-type [α/β-Mo 18 O 54 (SO 3 ) 2 ] 4- polyanions in the form of tetrapentylammonium salts were studied by a combination of IR, Raman and visible spectroscopy at high temperature and high pressure. Evidence of the formation of bronze-type materials above 400 K and also upon pressurization to 8 GPa is presented. This conclusion is suggested to be a general result for polyoxometalate compounds subjected to extreme conditions and it opens opportunities for the design of new materials with interesting optical and electronic properties. © 2011 Elsevier Inc.
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